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Limits of Resolution and Sensitivity of Proton Detected MAS Solid-State NMR Experiments at 111 kHz in Deuterated and Protonated Proteins
MAS solid-state NMR is capable of determining structures of protonated solid proteins using proton-detected experiments. These experiments are performed at MAS rotation frequency of around 110 kHz, employing 0.5 mg of material. Here, we compare (1)H, (13)C correlation spectra obtained from protonate...
Autores principales: | Xue, Kai, Sarkar, Riddhiman, Motz, Carina, Asami, Sam, Camargo, Diana C. Rodriguez, Decker, Venita, Wegner, Sebastian, Tosner, Zdenek, Reif, Bernd |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5547042/ https://www.ncbi.nlm.nih.gov/pubmed/28785098 http://dx.doi.org/10.1038/s41598-017-07253-1 |
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