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A phase transition caught in mid-course: independent and concomitant analyses of the monoclinic and triclinic structures of ((n)Bu(4)N)[Co(orotate)(2)(bipy)]·3H(2)O

The preparation and characterization of the (n)Bu(4)N(+) salts of two bis-orotate(2−) complexes of cobalt, namely bis­(tetra-n-butyl­ammonium) di­aqua­bis­(2,4-dioxo-1,2,3,4-tetra­hydro­pyrimidin-1-ide-6-carboxyl­ato-κ(2) N (1),O (6))cobalt(II) 1.8-hydrate, (C(16)H(36)N)(2)[Co(C(5)H(2)N(2)O(4))(2)(H...

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Detalles Bibliográficos
Autores principales: Castro, Miguel, Falvello, Larry R., Forcén-Vázquez, Elena, Guerra, Pablo, Al-Kenany, Nuha A., Martínez, Gema, Tomás, Milagros
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5601254/
https://www.ncbi.nlm.nih.gov/pubmed/28872072
http://dx.doi.org/10.1107/S2053229617010841