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Non-order–disorder allotwinning of the rhenium pincer complex cis-Re[(PNP(CH2)-iPr)(CO)(2)Cl]
Crystals of cis-Re[(PNP(CH2)-iPr)(CO)(2)Cl] (1) are made up of two geometrically non-equivalent polytypes with respective symmetries of P2(1)/c and I2/a. The structures were determined in a concurrent refinement, taking into account overlap of diffraction spots. The polytypes are composed of layers...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5628399/ https://www.ncbi.nlm.nih.gov/pubmed/28981000 http://dx.doi.org/10.1107/S205252061701006X |