Synthesis of a Novel Polyethoxysilsesquiazane and Thermal Conversion into Ternary Silicon Oxynitride Ceramics with Enhanced Thermal Stability

A novel polyethoxysilsesquiazane ([EtOSi(NH)(1.5)](n), EtOSZ) was synthesized by ammonolysis at −78 °C of ethoxytrichlorosilane (EtOSiCl(3)), which was isolated by distillation as a reaction product of SiCl(4) and EtOH. Attenuated total reflection-infra red (ATR-IR), (13)C-, and (29)Si-nuclear magne...

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Detalles Bibliográficos
Autores principales: Iwase, Yoshiaki, Horie, Yoji, Daiko, Yusuke, Honda, Sawao, Iwamoto, Yuji
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2017
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5744326/
https://www.ncbi.nlm.nih.gov/pubmed/29206217
http://dx.doi.org/10.3390/ma10121391

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5744326/
https://www.ncbi.nlm.nih.gov/pubmed/29206217
http://dx.doi.org/10.3390/ma10121391

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