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Synthesis of a Novel Polyethoxysilsesquiazane and Thermal Conversion into Ternary Silicon Oxynitride Ceramics with Enhanced Thermal Stability
A novel polyethoxysilsesquiazane ([EtOSi(NH)(1.5)](n), EtOSZ) was synthesized by ammonolysis at −78 °C of ethoxytrichlorosilane (EtOSiCl(3)), which was isolated by distillation as a reaction product of SiCl(4) and EtOH. Attenuated total reflection-infra red (ATR-IR), (13)C-, and (29)Si-nuclear magne...
| Autores principales: | , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
MDPI
2017
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5744326/ https://www.ncbi.nlm.nih.gov/pubmed/29206217 http://dx.doi.org/10.3390/ma10121391 |