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On-line coupling of derivatization with pre-concentration to determine trace levels of methotrexate

A new simple, sensitive and precise green analytical procedure using an automated packed-reactor derivatization technique coupled with on-line solid-phase enrichment (SPEn) has been developed and evaluated to determine trace levels of methotrexate (MTX). The method was based on injection of MTX into...

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Detalles Bibliográficos
Autores principales: Emara, Samy, Masujima, Tsutomu, Zarad, Walaa, Kamal, Maha, EL-Bagary, Ramzia
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5760918/
https://www.ncbi.nlm.nih.gov/pubmed/29403793
http://dx.doi.org/10.1016/j.jpha.2012.10.003