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A gel aging effect in the synthesis of open-framework gallium phosphates: structure solution and solid-state NMR of a large-pore, open-framework material
The templated zeolite-analogue GaPO-34 (CHA structure type) crystallises from a gel precursor Ga(2)O(3) : 2H(3)PO(4) : 1HF : 1.7SDA : 70H(2)O (where SDA = structure directing agent), treated hydrothermally for 24 hours at 170 °C using either pyridine or 1-methylimizadole as SDA and one of either poo...
Autores principales: | Broom, Lucy K., Clarkson, Guy J., Guillou, Nathalie, Hooper, Joseph E., Dawson, Daniel M., Tang, Chiu C., Ashbrook, Sharon E., Walton, Richard I. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Royal Society of Chemistry
2017
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5789431/ https://www.ncbi.nlm.nih.gov/pubmed/29171855 http://dx.doi.org/10.1039/c7dt03709k |
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