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Silane Reduction of 5-Hydroxy-6-methyl-pyridine-3,4-dicarboxylic Acid Diethyl Ester: Synthesis of Vitamin B(6)
Alternative methods for the synthesis of pyridoxine have been investigated. The key intermediate, 5-hydroxy-6-methyl-pyridine-3,4-dicarboxylic acid diethyl ester (5), was reduced with either a silane monomer (MeSiH(OEt)(2)) or a polysiloxane (polymethylhydrosiloxane, PMHS) to afford crude pyridoxine...
| Autores principales: | , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
MDPI
2003
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146842/ http://dx.doi.org/10.3390/81200873 |