Easy and Safe Preparations of (Diacetoxyiodo)arenes from Iodoarenes, with Urea-Hydrogen Peroxide Adduct (UHP) as the Oxidant and the Fully Interpreted (1)H- and (13)C-NMR Spectra of the Products †

An easy and safe, though only moderately effective method is presented for preparing (diacetoxyiodo)arenes, ArI(OAc)(2), from iodoarenes, ArI, using the commercially available and easily handled urea-hydrogen peroxide adduct (UHP) as the oxidant. The reactions take place in anhydrous AcOH/Ac(2)O/AcO...

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Detalles Bibliográficos
Autores principales: Zielinska, Agnieszka, Skulski, Lech
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2005
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6147544/
https://www.ncbi.nlm.nih.gov/pubmed/18007286
http://dx.doi.org/10.3390/10010190