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Chemical Synthesis of Deoxynivalenol-3-β-d-[(13)C(6)]-glucoside and Application in Stable Isotope Dilution Assays

Modified mycotoxins have been gaining importance in recent years and present a certain challenge in LC-MS/MS analysis. Due to the previous lack of a labeled isotopologue of the modified mycotoxin deoxynivalenol-3-glucoside, in our study we synthesized the first (13)C-labeled internal standard. There...

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Detalles Bibliográficos
Autores principales: Habler, Katharina, Frank, Oliver, Rychlik, Michael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2016
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6274488/
https://www.ncbi.nlm.nih.gov/pubmed/27355938
http://dx.doi.org/10.3390/molecules21070838