Cargando…
Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface
Ti-Al diffusion couples, prepared by resistance spot welding, were annealed up to 112 h at 823, 848, and 873 K in ambient atmosphere. The interfacial microstructure was observed and analyzed using SEM and TEM. The growth characterization of intermetallic compound formed at the Ti/Al solid state inte...
Autores principales: | , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2019
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6384985/ https://www.ncbi.nlm.nih.gov/pubmed/30720709 http://dx.doi.org/10.3390/ma12030472 |
_version_ | 1783397104531537920 |
---|---|
author | Zhao, Yangyang Li, Jiuyong Qiu, Ranfeng Shi, Hongxin |
author_facet | Zhao, Yangyang Li, Jiuyong Qiu, Ranfeng Shi, Hongxin |
author_sort | Zhao, Yangyang |
collection | PubMed |
description | Ti-Al diffusion couples, prepared by resistance spot welding, were annealed up to 112 h at 823, 848, and 873 K in ambient atmosphere. The interfacial microstructure was observed and analyzed using SEM and TEM. The growth characterization of intermetallic compound formed at the Ti/Al solid state interface was investigated. Only TiAl(3) phase was detected in the interfacial zone, and its growth was governed by reaction-controlled mechanism in the previous period and by diffusion-controlled mechanism in the latter period. The activation energies were 198,019 and 122,770 J/mol for reaction-controlled and diffusion-controlled mechanism, respectively. |
format | Online Article Text |
id | pubmed-6384985 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-63849852019-02-23 Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface Zhao, Yangyang Li, Jiuyong Qiu, Ranfeng Shi, Hongxin Materials (Basel) Article Ti-Al diffusion couples, prepared by resistance spot welding, were annealed up to 112 h at 823, 848, and 873 K in ambient atmosphere. The interfacial microstructure was observed and analyzed using SEM and TEM. The growth characterization of intermetallic compound formed at the Ti/Al solid state interface was investigated. Only TiAl(3) phase was detected in the interfacial zone, and its growth was governed by reaction-controlled mechanism in the previous period and by diffusion-controlled mechanism in the latter period. The activation energies were 198,019 and 122,770 J/mol for reaction-controlled and diffusion-controlled mechanism, respectively. MDPI 2019-02-04 /pmc/articles/PMC6384985/ /pubmed/30720709 http://dx.doi.org/10.3390/ma12030472 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Zhao, Yangyang Li, Jiuyong Qiu, Ranfeng Shi, Hongxin Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title | Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title_full | Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title_fullStr | Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title_full_unstemmed | Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title_short | Growth Characterization of Intermetallic Compound at the Ti/Al Solid State Interface |
title_sort | growth characterization of intermetallic compound at the ti/al solid state interface |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6384985/ https://www.ncbi.nlm.nih.gov/pubmed/30720709 http://dx.doi.org/10.3390/ma12030472 |
work_keys_str_mv | AT zhaoyangyang growthcharacterizationofintermetalliccompoundatthetialsolidstateinterface AT lijiuyong growthcharacterizationofintermetalliccompoundatthetialsolidstateinterface AT qiuranfeng growthcharacterizationofintermetalliccompoundatthetialsolidstateinterface AT shihongxin growthcharacterizationofintermetalliccompoundatthetialsolidstateinterface |