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Synthesis and crystal structure of 1,3-di-tert-butyl-2-chloro-4,4-diphenyl-1,3,2λ(3),4-diazaphosphasiletidine
The chemical reaction of dilithium N,N′-di((t)butyl)-Si,Si-diphenylsilanediamide and PCl(3) yielded an off-white solid. Sublimation of the crude product under reduced pressure at elevated temperature gave colourless prismatic crystals of the title compound, C(20)H(28)ClN(2)PSi, which crystalliz...
| Autores principales: | , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2019
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6399688/ https://www.ncbi.nlm.nih.gov/pubmed/30867959 http://dx.doi.org/10.1107/S2056989019002627 |