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Spinning faster: protein NMR at MAS frequencies up to 126 kHz

We report linewidth and proton T(1), T(1ρ) and T(2)′ relaxation data of the model protein ubiquitin acquired at MAS frequencies up to 126 kHz. We find a predominantly linear improvement in linewidths and coherence decay times of protons with increasing spinning frequency in the range from 93 to 126 ...

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Detalles Bibliográficos
Autores principales: Penzel, Susanne, Oss, Andres, Org, Mai-Liis, Samoson, Ago, Böckmann, Anja, Ernst, Matthias, Meier, Beat H.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Netherlands 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6441448/
https://www.ncbi.nlm.nih.gov/pubmed/30680507
http://dx.doi.org/10.1007/s10858-018-0219-9