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Spinning faster: protein NMR at MAS frequencies up to 126 kHz
We report linewidth and proton T(1), T(1ρ) and T(2)′ relaxation data of the model protein ubiquitin acquired at MAS frequencies up to 126 kHz. We find a predominantly linear improvement in linewidths and coherence decay times of protons with increasing spinning frequency in the range from 93 to 126 ...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer Netherlands
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6441448/ https://www.ncbi.nlm.nih.gov/pubmed/30680507 http://dx.doi.org/10.1007/s10858-018-0219-9 |