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HPLC purification technique: synthesis of unsymmetrical thiobarbituric acids

Synthesis of thiobarbituric acids by the reaction of 1,3-disubstituted thioureas and malonic acid in acetyl chloride-acetic acid medium and synthesis of cyclized pyrimidin-7-one by the interaction of 1-(2-hydroxyethyl)-aryl thioureas, with malonic acid in p-tolyl sulphonic acid and acetyl chloride-a...

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Detalles Bibliográficos
Autores principales: Deotale, Vinod D., Katiya, Manish M., Dhonde, Madhukar G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6664147/
https://www.ncbi.nlm.nih.gov/pubmed/31384677
http://dx.doi.org/10.1016/j.heliyon.2019.e02008