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Preparation of cubic Na(3)PS(4) by liquid-phase shaking in methyl acetate medium

Cubic Na(3)PS(4) (c-Na(3)PS(4)), a high temperature phase of Na(3)PS(4), is successfully prepared by liquid-phase shaking from Na(2)S and P(2)S(5) in methyl acetate medium. The effects of the amount of solvents, Na(2)S and heat treatment on the formation of c-Na(3)PS(4) are carefully investigated. I...

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Detalles Bibliográficos
Autores principales: Atsunori, Matsuda, Hirotada, Gamo, Phuc, Nguyen Huu Huy
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6859230/
https://www.ncbi.nlm.nih.gov/pubmed/31763471
http://dx.doi.org/10.1016/j.heliyon.2019.e02760