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Improved Access to Organo‐Soluble Di‐ and Tetrafluoridochlorate(I)/(III) Salts
A facile one‐pot gram‐scale synthesis of tetraalkylammonium tetrafluoridochlorate(III) [cat][ClF(4)] ([cat]=[NEt(3)Me](+), [NEt(4)](+)) is described. An acetonitrile solution of the corresponding alkylammonium chloride salt is fluorinated with diluted fluorine at low temperatures. The reaction proce...
| Autores principales: | , , , , , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
John Wiley and Sons Inc.
2020
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7540313/ https://www.ncbi.nlm.nih.gov/pubmed/32459871 http://dx.doi.org/10.1002/anie.202006268 |