Unexpected synthesis and crystal structure of N-{2-[2-(2-acetyl­ethen­yl)phen­oxy]eth­yl}-N-ethenyl-4-methyl­benzene­sulfonamide

The title compound, C(21)H(23)NO(4)S, obtained by alkaline treatment of 1,5-bis­(1-phen­oxy)-3-aza­pentane at moderate heating, is a N-tosyl­ated secondary vinyl­amine. An intra­molecular S=O⋯H—C hydrogen bond generates a 13-membered ring. The benzalacetone moiety adopts a trans conformation with re...

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Detalles Bibliográficos
Autores principales: Temesgen, Ayalew W., Luong, Minh Duc, Truong, Hong Hieu, Nguyen, Van Tuyen, Dang, Thi Tuyet Anh, Le, Tuan Anh, Tskhovrebov, Alexander G., Khrustalev, Victor N.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2020
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7784650/
https://www.ncbi.nlm.nih.gov/pubmed/33520267
http://dx.doi.org/10.1107/S2056989020015194

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7784650/
https://www.ncbi.nlm.nih.gov/pubmed/33520267
http://dx.doi.org/10.1107/S2056989020015194

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