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Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential

This work provides an analysis of X-ray micro computed tomography data of Sn-xBi solders with x = 20, 30, 35, 47, 58 wt.% Bi. The eutectic thickness, fraction of eutectic and primary phase are analyzed. Furthermore, the 3D data is evaluated by means of morphology parameters, such as, shape complexit...

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Autores principales: Siroky, Georg, Kraker, Elke, Rosc, Jördis, Kieslinger, Dietmar, Brunner, Roland, van der Zwaag, Sybrand, Kozeschnik, Ernst, Ecker, Werner
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7794811/
https://www.ncbi.nlm.nih.gov/pubmed/33396361
http://dx.doi.org/10.3390/ma14010153
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author Siroky, Georg
Kraker, Elke
Rosc, Jördis
Kieslinger, Dietmar
Brunner, Roland
van der Zwaag, Sybrand
Kozeschnik, Ernst
Ecker, Werner
author_facet Siroky, Georg
Kraker, Elke
Rosc, Jördis
Kieslinger, Dietmar
Brunner, Roland
van der Zwaag, Sybrand
Kozeschnik, Ernst
Ecker, Werner
author_sort Siroky, Georg
collection PubMed
description This work provides an analysis of X-ray micro computed tomography data of Sn-xBi solders with x = 20, 30, 35, 47, 58 wt.% Bi. The eutectic thickness, fraction of eutectic and primary phase are analyzed. Furthermore, the 3D data is evaluated by means of morphology parameters, such as, shape complexity, flatness, elongation and mean intercept length tensor. The investigated alloys are categorized in three groups based on their morphology, which are described as “complex dominant”, “complex- equiaxed” and “mixed”. The mechanical behavior of Sn-Bi alloys in the semi-solid configuration and the correlation with microstructural parameters are discussed. A varying degree of geometric anisotropy of the investigated alloys is found through the mean intercept length tensor. Representative volume element models for finite element simulations (RVE-FEM) are created from tomography data of each alloy to analyze a correlation of geometric and elastic anisotropy. The simulations reveal an elastic isotropic behavior due to the small difference of elastic constants of primary and eutectic phase. A discussion of properties in the semi-solid state and liquid phase healing is provided.
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spelling pubmed-77948112021-01-10 Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential Siroky, Georg Kraker, Elke Rosc, Jördis Kieslinger, Dietmar Brunner, Roland van der Zwaag, Sybrand Kozeschnik, Ernst Ecker, Werner Materials (Basel) Article This work provides an analysis of X-ray micro computed tomography data of Sn-xBi solders with x = 20, 30, 35, 47, 58 wt.% Bi. The eutectic thickness, fraction of eutectic and primary phase are analyzed. Furthermore, the 3D data is evaluated by means of morphology parameters, such as, shape complexity, flatness, elongation and mean intercept length tensor. The investigated alloys are categorized in three groups based on their morphology, which are described as “complex dominant”, “complex- equiaxed” and “mixed”. The mechanical behavior of Sn-Bi alloys in the semi-solid configuration and the correlation with microstructural parameters are discussed. A varying degree of geometric anisotropy of the investigated alloys is found through the mean intercept length tensor. Representative volume element models for finite element simulations (RVE-FEM) are created from tomography data of each alloy to analyze a correlation of geometric and elastic anisotropy. The simulations reveal an elastic isotropic behavior due to the small difference of elastic constants of primary and eutectic phase. A discussion of properties in the semi-solid state and liquid phase healing is provided. MDPI 2020-12-31 /pmc/articles/PMC7794811/ /pubmed/33396361 http://dx.doi.org/10.3390/ma14010153 Text en © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Siroky, Georg
Kraker, Elke
Rosc, Jördis
Kieslinger, Dietmar
Brunner, Roland
van der Zwaag, Sybrand
Kozeschnik, Ernst
Ecker, Werner
Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title_full Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title_fullStr Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title_full_unstemmed Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title_short Analysis of Sn-Bi Solders: X-ray Micro Computed Tomography Imaging and Microstructure Characterization in Relation to Properties and Liquid Phase Healing Potential
title_sort analysis of sn-bi solders: x-ray micro computed tomography imaging and microstructure characterization in relation to properties and liquid phase healing potential
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7794811/
https://www.ncbi.nlm.nih.gov/pubmed/33396361
http://dx.doi.org/10.3390/ma14010153
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