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High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target

High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mix...

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Autores principales: Winnicki, Marcin, Wiatrowski, Artur, Mazur, Michał
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7961378/
https://www.ncbi.nlm.nih.gov/pubmed/33807798
http://dx.doi.org/10.3390/ma14051228
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author Winnicki, Marcin
Wiatrowski, Artur
Mazur, Michał
author_facet Winnicki, Marcin
Wiatrowski, Artur
Mazur, Michał
author_sort Winnicki, Marcin
collection PubMed
description High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mixed in a volume ratio of 3:1. Composite In(2)O(3)/Sn coating had a mean thickness of 900 µm. HiPIMS process was performed in various mixtures of Ar:O(2): (i) 100:0 vol.%, (ii) 90:10 vol.%, (iii) 75:25 vol.%, (iv) 50:50 vol.%, and (v) 0:100 vol.%. Oxygen rich atmosphere was necessary to oxidize tin atoms. Self-design, simple high voltage power switch capable of charging the 20 µF capacitor bank from external high voltage power supply worked as a power supply for an unbalanced magnetron source. ITO thin films with thickness in the range of 30–40 nm were obtained after 300 deposition pulses of 900 V and deposition time of 900 s. The highest transmission of 88% at λ = 550 nm provided 0:100 vol. % Ar:O(2) mixture, together with the lowest resistivity of 0.03 Ω·cm.
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spelling pubmed-79613782021-03-17 High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target Winnicki, Marcin Wiatrowski, Artur Mazur, Michał Materials (Basel) Article High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mixed in a volume ratio of 3:1. Composite In(2)O(3)/Sn coating had a mean thickness of 900 µm. HiPIMS process was performed in various mixtures of Ar:O(2): (i) 100:0 vol.%, (ii) 90:10 vol.%, (iii) 75:25 vol.%, (iv) 50:50 vol.%, and (v) 0:100 vol.%. Oxygen rich atmosphere was necessary to oxidize tin atoms. Self-design, simple high voltage power switch capable of charging the 20 µF capacitor bank from external high voltage power supply worked as a power supply for an unbalanced magnetron source. ITO thin films with thickness in the range of 30–40 nm were obtained after 300 deposition pulses of 900 V and deposition time of 900 s. The highest transmission of 88% at λ = 550 nm provided 0:100 vol. % Ar:O(2) mixture, together with the lowest resistivity of 0.03 Ω·cm. MDPI 2021-03-05 /pmc/articles/PMC7961378/ /pubmed/33807798 http://dx.doi.org/10.3390/ma14051228 Text en © 2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Winnicki, Marcin
Wiatrowski, Artur
Mazur, Michał
High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title_full High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title_fullStr High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title_full_unstemmed High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title_short High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
title_sort high power impulse magnetron sputtering of in(2)o(3)/sn cold sprayed composite target
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7961378/
https://www.ncbi.nlm.nih.gov/pubmed/33807798
http://dx.doi.org/10.3390/ma14051228
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