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High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target
High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mix...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2021
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7961378/ https://www.ncbi.nlm.nih.gov/pubmed/33807798 http://dx.doi.org/10.3390/ma14051228 |
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author | Winnicki, Marcin Wiatrowski, Artur Mazur, Michał |
author_facet | Winnicki, Marcin Wiatrowski, Artur Mazur, Michał |
author_sort | Winnicki, Marcin |
collection | PubMed |
description | High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mixed in a volume ratio of 3:1. Composite In(2)O(3)/Sn coating had a mean thickness of 900 µm. HiPIMS process was performed in various mixtures of Ar:O(2): (i) 100:0 vol.%, (ii) 90:10 vol.%, (iii) 75:25 vol.%, (iv) 50:50 vol.%, and (v) 0:100 vol.%. Oxygen rich atmosphere was necessary to oxidize tin atoms. Self-design, simple high voltage power switch capable of charging the 20 µF capacitor bank from external high voltage power supply worked as a power supply for an unbalanced magnetron source. ITO thin films with thickness in the range of 30–40 nm were obtained after 300 deposition pulses of 900 V and deposition time of 900 s. The highest transmission of 88% at λ = 550 nm provided 0:100 vol. % Ar:O(2) mixture, together with the lowest resistivity of 0.03 Ω·cm. |
format | Online Article Text |
id | pubmed-7961378 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-79613782021-03-17 High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target Winnicki, Marcin Wiatrowski, Artur Mazur, Michał Materials (Basel) Article High Power Impulse Magnetron Sputtering (HiPIMS) was used for deposition of indium tin oxide (ITO) transparent thin films at low substrate temperature. A hybrid-type composite target was self-prepared by low-pressure cold spraying process. Prior to spraying In(2)O(3) and oxidized Sn powders were mixed in a volume ratio of 3:1. Composite In(2)O(3)/Sn coating had a mean thickness of 900 µm. HiPIMS process was performed in various mixtures of Ar:O(2): (i) 100:0 vol.%, (ii) 90:10 vol.%, (iii) 75:25 vol.%, (iv) 50:50 vol.%, and (v) 0:100 vol.%. Oxygen rich atmosphere was necessary to oxidize tin atoms. Self-design, simple high voltage power switch capable of charging the 20 µF capacitor bank from external high voltage power supply worked as a power supply for an unbalanced magnetron source. ITO thin films with thickness in the range of 30–40 nm were obtained after 300 deposition pulses of 900 V and deposition time of 900 s. The highest transmission of 88% at λ = 550 nm provided 0:100 vol. % Ar:O(2) mixture, together with the lowest resistivity of 0.03 Ω·cm. MDPI 2021-03-05 /pmc/articles/PMC7961378/ /pubmed/33807798 http://dx.doi.org/10.3390/ma14051228 Text en © 2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Winnicki, Marcin Wiatrowski, Artur Mazur, Michał High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title | High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title_full | High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title_fullStr | High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title_full_unstemmed | High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title_short | High Power Impulse Magnetron Sputtering of In(2)O(3)/Sn Cold Sprayed Composite Target |
title_sort | high power impulse magnetron sputtering of in(2)o(3)/sn cold sprayed composite target |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7961378/ https://www.ncbi.nlm.nih.gov/pubmed/33807798 http://dx.doi.org/10.3390/ma14051228 |
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