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A chromatography-free and aqueous waste-free process for thioamide preparation with Lawesson’s reagent

After completing the thio-substitution with Lawesson’s reagent, ethanol was found to be effective in the decomposition of the inherent stoichiometric six-membered-ring byproduct from the Lawesson’s reagent to a highly polarized diethyl thiophosphonate. The treatment significantly simplified the foll...

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Detalles Bibliográficos
Autores principales: Wu, Ke, Ling, Yichen, Ding, An, Jin, Liqun, Sun, Nan, Hu, Baoxiang, Shen, Zhenlu, Hu, Xinquan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8042485/
https://www.ncbi.nlm.nih.gov/pubmed/33889221
http://dx.doi.org/10.3762/bjoc.17.69