Cargando…
A chromatography-free and aqueous waste-free process for thioamide preparation with Lawesson’s reagent
After completing the thio-substitution with Lawesson’s reagent, ethanol was found to be effective in the decomposition of the inherent stoichiometric six-membered-ring byproduct from the Lawesson’s reagent to a highly polarized diethyl thiophosphonate. The treatment significantly simplified the foll...
| Autores principales: | , , , , , , , |
|---|---|
| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
Beilstein-Institut
2021
|
| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8042485/ https://www.ncbi.nlm.nih.gov/pubmed/33889221 http://dx.doi.org/10.3762/bjoc.17.69 |