GC-MS Discrimination of Citrulline from Ornithine and Homocitrulline from Lysine by Chemical Derivatization: Evidence of Formation of N(5)-Carboxy-ornithine and N(6)-Carboxy-lysine

Derivatization of amino acids by 2 M HCl/CH(3)OH (60 min, 80 °C) followed by derivatization of the intermediate methyl esters with pentafluoropropionic anhydride (PFPA) in ethyl acetate (30 min, 65 °C) is a useful two-step derivatization procedure (procedure A) for their quantitative measurement in...

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Detalles Bibliográficos
Autores principales: Baskal, Svetlana, Bollenbach, Alexander, Tsikas, Dimitrios
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8071523/
https://www.ncbi.nlm.nih.gov/pubmed/33921162
http://dx.doi.org/10.3390/molecules26082301

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8071523/
https://www.ncbi.nlm.nih.gov/pubmed/33921162
http://dx.doi.org/10.3390/molecules26082301

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