Development of a rapid GC-FID method to simultaneously determine triethylamine, diisopropylamine, and 1,1,3,3-tetramethylguanidine residues in an active pharmaceutical ingredient

A rapid GC-FID method was developed to simultaneously determine residual levels of triethylamine (TEA), 1,1,3,3-tetramethylguanidine (TMG), and diisopropylamine (DIPA) in the synthetic route of an active pharmaceutical ingredient (API). Due to the severe absorption of amines on GC stationary phases,...

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Detalles Bibliográficos
Autores principales: Shou, Minshan, Qiu, Haixiao
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Xi'an Jiaotong University 2021
Materias:
Short Communication
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8116200/
https://www.ncbi.nlm.nih.gov/pubmed/34012701
http://dx.doi.org/10.1016/j.jpha.2020.06.007

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8116200/
https://www.ncbi.nlm.nih.gov/pubmed/34012701
http://dx.doi.org/10.1016/j.jpha.2020.06.007

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