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Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham

Dry-cured Iberian ham is officially classified into different commercial categories according to the pig’s breed and feeding regime. These reach very different prices, thus promoting labelling fraud and causing great damage to the food sector. In this work, a method based on Raman spectroscopy was e...

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Autores principales: Martín-Gómez, Andrés, Arroyo-Manzanares, Natalia, García-Nicolás, María, López-Lorente, Ángela I., Cárdenas, Soledad, López-García, Ignacio, Viñas, Pilar, Hernández-Córdoba, Manuel, Arce, Lourdes
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8225093/
https://www.ncbi.nlm.nih.gov/pubmed/34073727
http://dx.doi.org/10.3390/foods10061177
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author Martín-Gómez, Andrés
Arroyo-Manzanares, Natalia
García-Nicolás, María
López-Lorente, Ángela I.
Cárdenas, Soledad
López-García, Ignacio
Viñas, Pilar
Hernández-Córdoba, Manuel
Arce, Lourdes
author_facet Martín-Gómez, Andrés
Arroyo-Manzanares, Natalia
García-Nicolás, María
López-Lorente, Ángela I.
Cárdenas, Soledad
López-García, Ignacio
Viñas, Pilar
Hernández-Córdoba, Manuel
Arce, Lourdes
author_sort Martín-Gómez, Andrés
collection PubMed
description Dry-cured Iberian ham is officially classified into different commercial categories according to the pig’s breed and feeding regime. These reach very different prices, thus promoting labelling fraud and causing great damage to the food sector. In this work, a method based on Raman spectroscopy was explored as a rapid in situ screening tool for Iberian ham samples. A total of 110 samples were analyzed to assess the potential of this technique to differentiate purebred, crossbred, acorn-fed and feed-fed dry-cured Iberian ham. A continuous signal probably due to sample fluorescence was obtained, which hid the Raman scattering signal. Therefore, chemometric treatment was applied in order to extract non-apparent information. High validated classification rates were obtained for feeding regime (83.3%) and breed (86.7%). In addition, an interlaboratory study was carried out to confirm the applicability of the method with 52 samples, obtaining a validated rate above 80%.
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spelling pubmed-82250932021-06-25 Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham Martín-Gómez, Andrés Arroyo-Manzanares, Natalia García-Nicolás, María López-Lorente, Ángela I. Cárdenas, Soledad López-García, Ignacio Viñas, Pilar Hernández-Córdoba, Manuel Arce, Lourdes Foods Article Dry-cured Iberian ham is officially classified into different commercial categories according to the pig’s breed and feeding regime. These reach very different prices, thus promoting labelling fraud and causing great damage to the food sector. In this work, a method based on Raman spectroscopy was explored as a rapid in situ screening tool for Iberian ham samples. A total of 110 samples were analyzed to assess the potential of this technique to differentiate purebred, crossbred, acorn-fed and feed-fed dry-cured Iberian ham. A continuous signal probably due to sample fluorescence was obtained, which hid the Raman scattering signal. Therefore, chemometric treatment was applied in order to extract non-apparent information. High validated classification rates were obtained for feeding regime (83.3%) and breed (86.7%). In addition, an interlaboratory study was carried out to confirm the applicability of the method with 52 samples, obtaining a validated rate above 80%. MDPI 2021-05-24 /pmc/articles/PMC8225093/ /pubmed/34073727 http://dx.doi.org/10.3390/foods10061177 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Martín-Gómez, Andrés
Arroyo-Manzanares, Natalia
García-Nicolás, María
López-Lorente, Ángela I.
Cárdenas, Soledad
López-García, Ignacio
Viñas, Pilar
Hernández-Córdoba, Manuel
Arce, Lourdes
Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title_full Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title_fullStr Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title_full_unstemmed Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title_short Portable Raman Spectrometer as a Screening Tool for Characterization of Iberian Dry-Cured Ham
title_sort portable raman spectrometer as a screening tool for characterization of iberian dry-cured ham
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8225093/
https://www.ncbi.nlm.nih.gov/pubmed/34073727
http://dx.doi.org/10.3390/foods10061177
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