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Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography

X-ray topography defect analysis of entire 1.8-inch GaN substrates, using the Borrmann effect, is presented in this paper. The GaN wafers were grown by the ammonothermal method. Borrmann effect topography of anomalous transmission could be applied due to the low defect density of the substrates. It...

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Autores principales: Kirste, Lutz, Grabianska, Karolina, Kucharski, Robert, Sochacki, Tomasz, Lucznik, Boleslaw, Bockowski, Michal
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2021
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8509523/
https://www.ncbi.nlm.nih.gov/pubmed/34639870
http://dx.doi.org/10.3390/ma14195472
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author Kirste, Lutz
Grabianska, Karolina
Kucharski, Robert
Sochacki, Tomasz
Lucznik, Boleslaw
Bockowski, Michal
author_facet Kirste, Lutz
Grabianska, Karolina
Kucharski, Robert
Sochacki, Tomasz
Lucznik, Boleslaw
Bockowski, Michal
author_sort Kirste, Lutz
collection PubMed
description X-ray topography defect analysis of entire 1.8-inch GaN substrates, using the Borrmann effect, is presented in this paper. The GaN wafers were grown by the ammonothermal method. Borrmann effect topography of anomalous transmission could be applied due to the low defect density of the substrates. It was possible to trace the process and growth history of the GaN crystals in detail from their defect pattern imaged. Microscopic defects such as threading dislocations, but also macroscopic defects, for example dislocation clusters due to preparation insufficiency, traces of facet formation, growth bands, dislocation walls and dislocation bundles, were detected. Influences of seed crystal preparation and process parameters of crystal growth on the formation of the defects are discussed.
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spelling pubmed-85095232021-10-13 Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography Kirste, Lutz Grabianska, Karolina Kucharski, Robert Sochacki, Tomasz Lucznik, Boleslaw Bockowski, Michal Materials (Basel) Article X-ray topography defect analysis of entire 1.8-inch GaN substrates, using the Borrmann effect, is presented in this paper. The GaN wafers were grown by the ammonothermal method. Borrmann effect topography of anomalous transmission could be applied due to the low defect density of the substrates. It was possible to trace the process and growth history of the GaN crystals in detail from their defect pattern imaged. Microscopic defects such as threading dislocations, but also macroscopic defects, for example dislocation clusters due to preparation insufficiency, traces of facet formation, growth bands, dislocation walls and dislocation bundles, were detected. Influences of seed crystal preparation and process parameters of crystal growth on the formation of the defects are discussed. MDPI 2021-09-22 /pmc/articles/PMC8509523/ /pubmed/34639870 http://dx.doi.org/10.3390/ma14195472 Text en © 2021 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kirste, Lutz
Grabianska, Karolina
Kucharski, Robert
Sochacki, Tomasz
Lucznik, Boleslaw
Bockowski, Michal
Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title_full Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title_fullStr Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title_full_unstemmed Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title_short Structural Analysis of Low Defect Ammonothermally Grown GaN Wafers by Borrmann Effect X-ray Topography
title_sort structural analysis of low defect ammonothermally grown gan wafers by borrmann effect x-ray topography
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8509523/
https://www.ncbi.nlm.nih.gov/pubmed/34639870
http://dx.doi.org/10.3390/ma14195472
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