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Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
[Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the fi...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
American Chemical
Society
2021
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8532148/ https://www.ncbi.nlm.nih.gov/pubmed/33847493 http://dx.doi.org/10.1021/acs.jafc.1c00622 |
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author | Gradišek, Anton Cifelli, Mario Ancora, Donatella Sepe, Ana Zalar, Boštjan Apih, Tomaž Domenici, Valentina |
author_facet | Gradišek, Anton Cifelli, Mario Ancora, Donatella Sepe, Ana Zalar, Boštjan Apih, Tomaž Domenici, Valentina |
author_sort | Gradišek, Anton |
collection | PubMed |
description | [Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the field of food characterization and authentication. In this study, we focused on relaxation times T(1) and T(2) measured at different magnetic field strengths (namely, 2, 100, and 400 MHz) and (1)H NMR T(1) relaxometry dispersions directly on olive oil samples without any chemical/physical treatments. A large set of EVOO samples produced in two regions of Italy, Tuscany and Apulia, were investigated by means of (1)H NMR relaxation techniques. The relaxation studies reported here show several common features between the two sets of EVOO samples, thus indicating that relaxation properties, namely, the ranges of values of T(1) and T(2) at 2 and 100 MHz, are characteristic of EVOOs, independently from the cultivars, climate, and geographic origin. This is a promising result in view of quality control and monitoring. |
format | Online Article Text |
id | pubmed-8532148 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2021 |
publisher | American Chemical
Society |
record_format | MEDLINE/PubMed |
spelling | pubmed-85321482021-10-22 Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements Gradišek, Anton Cifelli, Mario Ancora, Donatella Sepe, Ana Zalar, Boštjan Apih, Tomaž Domenici, Valentina J Agric Food Chem [Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the field of food characterization and authentication. In this study, we focused on relaxation times T(1) and T(2) measured at different magnetic field strengths (namely, 2, 100, and 400 MHz) and (1)H NMR T(1) relaxometry dispersions directly on olive oil samples without any chemical/physical treatments. A large set of EVOO samples produced in two regions of Italy, Tuscany and Apulia, were investigated by means of (1)H NMR relaxation techniques. The relaxation studies reported here show several common features between the two sets of EVOO samples, thus indicating that relaxation properties, namely, the ranges of values of T(1) and T(2) at 2 and 100 MHz, are characteristic of EVOOs, independently from the cultivars, climate, and geographic origin. This is a promising result in view of quality control and monitoring. American Chemical Society 2021-04-13 2021-10-20 /pmc/articles/PMC8532148/ /pubmed/33847493 http://dx.doi.org/10.1021/acs.jafc.1c00622 Text en © 2021 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by/4.0/Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Gradišek, Anton Cifelli, Mario Ancora, Donatella Sepe, Ana Zalar, Boštjan Apih, Tomaž Domenici, Valentina Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements |
title | Analysis of Extra Virgin Olive Oils from Two Italian
Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and
Relaxometry Measurements |
title_full | Analysis of Extra Virgin Olive Oils from Two Italian
Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and
Relaxometry Measurements |
title_fullStr | Analysis of Extra Virgin Olive Oils from Two Italian
Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and
Relaxometry Measurements |
title_full_unstemmed | Analysis of Extra Virgin Olive Oils from Two Italian
Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and
Relaxometry Measurements |
title_short | Analysis of Extra Virgin Olive Oils from Two Italian
Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and
Relaxometry Measurements |
title_sort | analysis of extra virgin olive oils from two italian
regions by means of proton nuclear magnetic resonance relaxation and
relaxometry measurements |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8532148/ https://www.ncbi.nlm.nih.gov/pubmed/33847493 http://dx.doi.org/10.1021/acs.jafc.1c00622 |
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