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Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements

[Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the fi...

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Autores principales: Gradišek, Anton, Cifelli, Mario, Ancora, Donatella, Sepe, Ana, Zalar, Boštjan, Apih, Tomaž, Domenici, Valentina
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2021
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8532148/
https://www.ncbi.nlm.nih.gov/pubmed/33847493
http://dx.doi.org/10.1021/acs.jafc.1c00622
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author Gradišek, Anton
Cifelli, Mario
Ancora, Donatella
Sepe, Ana
Zalar, Boštjan
Apih, Tomaž
Domenici, Valentina
author_facet Gradišek, Anton
Cifelli, Mario
Ancora, Donatella
Sepe, Ana
Zalar, Boštjan
Apih, Tomaž
Domenici, Valentina
author_sort Gradišek, Anton
collection PubMed
description [Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the field of food characterization and authentication. In this study, we focused on relaxation times T(1) and T(2) measured at different magnetic field strengths (namely, 2, 100, and 400 MHz) and (1)H NMR T(1) relaxometry dispersions directly on olive oil samples without any chemical/physical treatments. A large set of EVOO samples produced in two regions of Italy, Tuscany and Apulia, were investigated by means of (1)H NMR relaxation techniques. The relaxation studies reported here show several common features between the two sets of EVOO samples, thus indicating that relaxation properties, namely, the ranges of values of T(1) and T(2) at 2 and 100 MHz, are characteristic of EVOOs, independently from the cultivars, climate, and geographic origin. This is a promising result in view of quality control and monitoring.
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spelling pubmed-85321482021-10-22 Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements Gradišek, Anton Cifelli, Mario Ancora, Donatella Sepe, Ana Zalar, Boštjan Apih, Tomaž Domenici, Valentina J Agric Food Chem [Image: see text] The interest in development of new non-destructive methods for characterization of extra virgin olive oils (EVOOs) has been increasing in the recent years. Among different experimental techniques, nuclear magnetic resonance (NMR) relaxation measurements are very promising in the field of food characterization and authentication. In this study, we focused on relaxation times T(1) and T(2) measured at different magnetic field strengths (namely, 2, 100, and 400 MHz) and (1)H NMR T(1) relaxometry dispersions directly on olive oil samples without any chemical/physical treatments. A large set of EVOO samples produced in two regions of Italy, Tuscany and Apulia, were investigated by means of (1)H NMR relaxation techniques. The relaxation studies reported here show several common features between the two sets of EVOO samples, thus indicating that relaxation properties, namely, the ranges of values of T(1) and T(2) at 2 and 100 MHz, are characteristic of EVOOs, independently from the cultivars, climate, and geographic origin. This is a promising result in view of quality control and monitoring. American Chemical Society 2021-04-13 2021-10-20 /pmc/articles/PMC8532148/ /pubmed/33847493 http://dx.doi.org/10.1021/acs.jafc.1c00622 Text en © 2021 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by/4.0/Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Gradišek, Anton
Cifelli, Mario
Ancora, Donatella
Sepe, Ana
Zalar, Boštjan
Apih, Tomaž
Domenici, Valentina
Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title_full Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title_fullStr Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title_full_unstemmed Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title_short Analysis of Extra Virgin Olive Oils from Two Italian Regions by Means of Proton Nuclear Magnetic Resonance Relaxation and Relaxometry Measurements
title_sort analysis of extra virgin olive oils from two italian regions by means of proton nuclear magnetic resonance relaxation and relaxometry measurements
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8532148/
https://www.ncbi.nlm.nih.gov/pubmed/33847493
http://dx.doi.org/10.1021/acs.jafc.1c00622
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