Revealing the early stages of carbamazepine crystallization by cryoTEM and 3D electron diffraction

Time-resolved carbamazepine crystallization from wet ethanol has been monitored using a combination of cryoTEM and 3D electron diffraction. Carbamazepine is shown to crystallize exclusively as a dihydrate after 180 s. When the timescale was reduced to 30 s, three further polymorphs could be identifi...

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Detalles Bibliográficos
Autores principales: Broadhurst, Edward T., Xu, Hongyi, Parsons, Simon, Nudelman, Fabio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2021
Materias:
Research Letters
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8562671/
https://www.ncbi.nlm.nih.gov/pubmed/34804540
http://dx.doi.org/10.1107/S2052252521010101

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8562671/
https://www.ncbi.nlm.nih.gov/pubmed/34804540
http://dx.doi.org/10.1107/S2052252521010101

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