Cargando…

Poly(acrylamide-co-N,N′-methylenebisacrylamide) Monoliths for High-Peak-Capacity Hydrophilic-Interaction Chromatography–High-Resolution Mass Spectrometry of Intact Proteins at Low Trifluoroacetic Acid Content

[Image: see text] In this study, we optimized a polymerization mixture to synthesize poly(acrylamide-co-N,N′-methylenebisacrylamide) monolithic stationary phases for hydrophilic-interaction chromatography (HILIC) of intact proteins. Thermal polymerization was performed, and the effects of varying th...

Descripción completa

Detalles Bibliográficos
Autores principales:	Passamonti, Marta, de Roos, Chiem, Schoenmakers, Peter J., Gargano, Andrea F.G.
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	American Chemical Society 2021
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8655738/ https://www.ncbi.nlm.nih.gov/pubmed/34807576 http://dx.doi.org/10.1021/acs.analchem.1c03473

Ejemplares similares

A novel catalyst system for the synthesis of N,N′-Methylenebisacrylamide from acrylamide
por: Avşar, Abdullah, et al.
Publicado: (2017)

Reproductive toxicology. Methylenebisacrylamide.
Publicado: (1997)

Novel Grafted/Crosslinked Cellulose Acetate Membrane with N-isopropylacrylamide/N,N-methylenebisacrylamide for Water Desalination
por: Elkony, Yasmeen, et al.
Publicado: (2020)

Nanocurcumin and curcumin prevent N, N'-methylenebisacrylamide-induced liver damage and promotion of hepatic cancer cell growth
por: Atia, Mona M., et al.
Publicado: (2022)

Manipulation of the Glass Transition Properties of a High-Solid System Made of Acrylic Acid-N,N′-Methylenebisacrylamide Copolymer Grafted on Hydroxypropyl Methyl Cellulose
por: Nassar, Nazim, et al.
Publicado: (2021)

Prediction of Intact N-Glycopeptide Retention Time Windows in Hydrophilic Interaction Liquid Chromatography
por: Kozlik, Petr, et al.
Publicado: (2022)

Microfluidic ion stripper for removal of trifluoroacetic acid from mobile phases used in HILIC-MS of intact proteins
por: Wouters, Sam, et al.
Publicado: (2021)

Hyperbranched Glycopolymers of 2-(α-d-Mannopyranose) Ethyl Methacrylate and N,N’-Methylenebisacrylamide: Synthesis, Characterization and Multivalent Recognitions with Concanavalin A
por: Zhang, Yuangong, et al.
Publicado: (2018)

Characterization of Intact Neo-Glycoproteins by Hydrophilic Interaction Liquid Chromatography
por: Pedrali, Alice, et al.
Publicado: (2014)

Post-polymerization photografting on methacrylate-based monoliths for separation of intact proteins and protein digests with comprehensive two-dimensional liquid chromatography hyphenated with high-resolution mass spectrometry
por: Vonk, Rudy J., et al.
Publicado: (2015)

Confinement of Monolithic Stationary Phases in Targeted Regions of 3D-Printed Titanium Devices Using Thermal Polymerization
por: Passamonti, Marta, et al.
Publicado: (2019)

Assessment of cytotoxicity of (N-isopropyl acrylamide) and Poly(N-isopropyl acrylamide)-coated surfaces
por: Cooperstein, Marta A, et al.
Publicado: (2013)

Optimizing separations in online comprehensive two‐dimensional liquid chromatography
por: Pirok, Bob W.J., et al.
Publicado: (2017)

Reproductive toxicology. N-(hydroxymethyl)acrylamide.
Publicado: (1997)

l-Lysinium trifluoroacetate
por: Sun, Zhi Hua, et al.
Publicado: (2008)

N-Benzyl-N-(4-chlorophenyl)acrylamide
por: Hu, Yi-Min, et al.
Publicado: (2007)

Bis[N′-(3-cyanobenzylidene)isonicotinohydrazide]silver(I) trifluoroacetate
por: Niu, Cao-Yuan, et al.
Publicado: (2009)

Rapid fabrication of zwitterionic sulfobetaine vinylimidazole-based monoliths via photoinitiated copolymerization for hydrophilic interaction chromatography
por: Wang, Qiqin, et al.
Publicado: (2022)

In-Depth Performance Analysis and Comparison of Monolithic and Particulate Zwitterionic Hydrophilic Interaction Liquid Chromatography Polymer Columns
por: Li, Haibin, et al.
Publicado: (2023)

RAFT Emulsion Polymerization of Styrene Using a Poly((N,N-dimethyl acrylamide)-co-(N-isopropyl acrylamide)) mCTA: Synthesis and Thermosensitivity
por: Nieswandt, Katharina, et al.
Publicado: (2021)

2-Aminopyridinium trifluoroacetate
por: Hemamalini, Madhukar, et al.
Publicado: (2010)

Cytenamide trifluoroacetic acid solvate
por: Johnston, Andrea, et al.
Publicado: (2008)

Transparent and Robust All-Cellulose Nanocomposite Packaging Materials Prepared in a Mixture of Trifluoroacetic Acid and Trifluoroacetic Anhydride
por: Guzman-Puyol, Susana, et al.
Publicado: (2019)

Analysis using size exclusion chromatography of poly(N-isopropyl acrylamide) using methanol as an eluent
por: Swift, Thomas, et al.
Publicado: (2017)

Trifluoroacetic acid as excipient destabilizes melittin causing the selective aggregation of melittin within the centrin-melittin-trifluoroacetic acid complexa)
por: Pastrana-Rios, Belinda, et al.
Publicado: (2015)

(Acetato-κ(2) O,O′)bis(1,10-phenanthroline-κ(2) N,N′)copper(II) trifluoroacetate tetrahydrate
por: Wang, Jinxia, et al.
Publicado: (2010)

Synthesis and antimicrobial activity of N-(indol-5-yl)trifluoroacetamides and indol-5-ylaminium trifluoroacetates substituted in the pyrrole ring
por: Yamashkin, S. A., et al.
Publicado: (2022)

Smart Hydrogels: Preparation, Characterization, and Determination of Transition Points of Crosslinked N-Isopropyl Acrylamide/Acrylamide/Carboxylic Acids Polymers
por: Işıkver, Yasemin, et al.
Publicado: (2021)

Synthesis, Characterization and Antibacterial Application of Copolymers Based on N,N-Dimethyl Acrylamide and Acrylic Acid
por: Nakan, Ulantay, et al.
Publicado: (2021)

(R)-1-Phenylethylammonium trifluoroacetate
por: Hernández Linares, María-Guadalupe, et al.
Publicado: (2010)

2-Amino-5-bromopyridinium trifluoroacetate
por: Hemamalini, Madhukar, et al.
Publicado: (2010)

2-Amino-5-chloropyridinium trifluoroacetate
por: Hemamalini, Madhukar, et al.
Publicado: (2010)

2-Amino-4-methylpyridinium trifluoroacetate
por: Hemamalini, Madhukar, et al.
Publicado: (2010)

2-Amino-5-methylpyridinium trifluoroacetate
por: Thanigaimani, Kaliyaperumal, et al.
Publicado: (2012)

Predicting retention time in hydrophilic interaction liquid chromatography mass spectrometry and its use for peak annotation in metabolomics
por: Cao, Mingshu, et al.
Publicado: (2014)

Synthesis of Thermo-Responsive Polymer via Radical (Co)polymerization of N,N-Dimethyl-α-(hydroxymethyl)acrylamide with N,N-Diethylacrylamide
por: Kohsaka, Yasuhiro, et al.
Publicado: (2016)

Therapeutic potential of N-acetylcysteine in acrylamide acute neurotoxicity in adult zebrafish
por: Faria, Melissa, et al.
Publicado: (2019)

Branched amphotericin functional poly(N-isopropyl acrylamide): an antifungal polymer
por: Swift, Thomas, et al.
Publicado: (2021)

Ambient Pressure Hybrid Silica Monoliths with Hexamethyldisilazane: From Vitreous Hydrophilic Xerogels to Superhydrophobic Aerogels
por: Júlio, Maria de Fátima, et al.
Publicado: (2017)

Maltose-Functionalized Hydrophilic Magnetic Nanoparticles with Polymer Brushes for Highly Selective Enrichment of N-Linked Glycopeptides
por: Bi, Changfen, et al.
Publicado: (2018)

Cannot write session to /tmp/vufind_sessions/sess_bfjblsggs8cea58s4v9bkibp5o