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Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector

The latest Complementary Metal Oxide Semiconductor (CMOS) 2D sensors now rival the performance of state-of-the-art photon detectors for optical application, combining a high-frame-rate speed with a wide dynamic range. While the advent of high-repetition-rate hard X-ray free-electron lasers (FELs) ha...

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Autores principales: Léveillé, Cyril, Desjardins, Kewin, Popescu, Horia, Vondungbo, Boris, Hennes, Marcel, Delaunay, Renaud, Jal, Emmanuelle, De Angelis, Dario, Pancaldi, Matteo, Pedersoli, Emanuele, Capotondi, Flavio, Jaouen, Nicolas
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8733974/
https://www.ncbi.nlm.nih.gov/pubmed/34985427
http://dx.doi.org/10.1107/S1600577521012303
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author Léveillé, Cyril
Desjardins, Kewin
Popescu, Horia
Vondungbo, Boris
Hennes, Marcel
Delaunay, Renaud
Jal, Emmanuelle
De Angelis, Dario
Pancaldi, Matteo
Pedersoli, Emanuele
Capotondi, Flavio
Jaouen, Nicolas
author_facet Léveillé, Cyril
Desjardins, Kewin
Popescu, Horia
Vondungbo, Boris
Hennes, Marcel
Delaunay, Renaud
Jal, Emmanuelle
De Angelis, Dario
Pancaldi, Matteo
Pedersoli, Emanuele
Capotondi, Flavio
Jaouen, Nicolas
author_sort Léveillé, Cyril
collection PubMed
description The latest Complementary Metal Oxide Semiconductor (CMOS) 2D sensors now rival the performance of state-of-the-art photon detectors for optical application, combining a high-frame-rate speed with a wide dynamic range. While the advent of high-repetition-rate hard X-ray free-electron lasers (FELs) has boosted the development of com­plex large-area fast CCD detectors in the extreme ultraviolet (EUV) and soft X-ray domains, scientists lacked such high-performance 2D detectors, principally due to the very poor efficiency limited by the sensor processing. Recently, a new generation of large back-side-illuminated scientific CMOS sensors (CMOS-BSI) has been developed and commercialized. One of these cost-efficient and com­petitive sensors, the GSENSE400BSI, has been implemented and characterized, and the proof of concept has been carried out at a synchrotron or laser-based X-ray source. In this article, we explore the feasibility of single-shot ultra-fast ex­peri­ments at FEL sources operating in the EUV/soft X-ray regime with an AXIS-SXR camera equipped with the GSENSE400BSI-TVISB sensor. We illustrate the detector capabilities by performing a soft X-ray magnetic scattering experiment at the DiProi end-station of the FERMI FEL. These measurements show the possibility of integrating this camera for collecting single-shot images at the 50 Hz operation mode of FERMI with a cropped image size of 700 × 700 pixels. The efficiency of the sensor at a working photon energy of 58 eV and the linearity over the large FEL intensity have been verified. Moreover, on-the-fly time-resolved single-shot X-ray resonant magnetic scattering imaging from prototype Co/Pt multilayer films has been carried out with a time collection gain of 30 com­pared to the classical start-and-stop acquisition method performed with the conventional CCD-BSI detector available at the end-station.
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spelling pubmed-87339742022-01-19 Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector Léveillé, Cyril Desjardins, Kewin Popescu, Horia Vondungbo, Boris Hennes, Marcel Delaunay, Renaud Jal, Emmanuelle De Angelis, Dario Pancaldi, Matteo Pedersoli, Emanuele Capotondi, Flavio Jaouen, Nicolas J Synchrotron Radiat Research Papers The latest Complementary Metal Oxide Semiconductor (CMOS) 2D sensors now rival the performance of state-of-the-art photon detectors for optical application, combining a high-frame-rate speed with a wide dynamic range. While the advent of high-repetition-rate hard X-ray free-electron lasers (FELs) has boosted the development of com­plex large-area fast CCD detectors in the extreme ultraviolet (EUV) and soft X-ray domains, scientists lacked such high-performance 2D detectors, principally due to the very poor efficiency limited by the sensor processing. Recently, a new generation of large back-side-illuminated scientific CMOS sensors (CMOS-BSI) has been developed and commercialized. One of these cost-efficient and com­petitive sensors, the GSENSE400BSI, has been implemented and characterized, and the proof of concept has been carried out at a synchrotron or laser-based X-ray source. In this article, we explore the feasibility of single-shot ultra-fast ex­peri­ments at FEL sources operating in the EUV/soft X-ray regime with an AXIS-SXR camera equipped with the GSENSE400BSI-TVISB sensor. We illustrate the detector capabilities by performing a soft X-ray magnetic scattering experiment at the DiProi end-station of the FERMI FEL. These measurements show the possibility of integrating this camera for collecting single-shot images at the 50 Hz operation mode of FERMI with a cropped image size of 700 × 700 pixels. The efficiency of the sensor at a working photon energy of 58 eV and the linearity over the large FEL intensity have been verified. Moreover, on-the-fly time-resolved single-shot X-ray resonant magnetic scattering imaging from prototype Co/Pt multilayer films has been carried out with a time collection gain of 30 com­pared to the classical start-and-stop acquisition method performed with the conventional CCD-BSI detector available at the end-station. International Union of Crystallography 2022-01-01 /pmc/articles/PMC8733974/ /pubmed/34985427 http://dx.doi.org/10.1107/S1600577521012303 Text en © Lveillé et al. 2022 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Léveillé, Cyril
Desjardins, Kewin
Popescu, Horia
Vondungbo, Boris
Hennes, Marcel
Delaunay, Renaud
Jal, Emmanuelle
De Angelis, Dario
Pancaldi, Matteo
Pedersoli, Emanuele
Capotondi, Flavio
Jaouen, Nicolas
Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title_full Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title_fullStr Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title_full_unstemmed Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title_short Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector
title_sort single-shot experiments at the soft x-fel fermi using a back-side-illuminated scientific cmos detector
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8733974/
https://www.ncbi.nlm.nih.gov/pubmed/34985427
http://dx.doi.org/10.1107/S1600577521012303
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