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Redetermination of the structure of 2-amino-8-thia-1,5-diazaspiro[4.5]dec-1-en-5-ium chloride monohydrate
The reaction of β-(thiomorpholin-1-yl)propioamidoxime with tosyl chloride in CHCl(3) in the presence of DIPEA when heated at 343 K for 8 h afforded the title hydrated salt, C(7)H(14)N(3)S(+)·Cl(−)·H(2)O, in 84% yield. This course of the tosylation reaction differs from the result of tosylation o...
| Autores principales: | , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
International Union of Crystallography
2022
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8819427/ https://www.ncbi.nlm.nih.gov/pubmed/35145744 http://dx.doi.org/10.1107/S2056989022000111 |