Cargando…

Redetermination of the structure of 2-amino-8-thia-1,5-diazaspiro[4.5]dec-1-en-5-ium chloride monohydrate

The reaction of β-(thiomorpholin-1-yl)propioamidoxime with tosyl chloride in CHCl(3) in the presence of DIPEA when heated at 343 K for 8 h afforded the title hydrated salt, C(7)H(14)N(3)S(+)·Cl(−)·H(2)O, in 84% yield. This course of the tosylation reaction differs from the result of tosylation o...

Descripción completa

Detalles Bibliográficos
Autores principales:	Kayukova, Lyudmila A., Yergaliyeva, Elmira M., Vologzhanina, Anna V.
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	International Union of Crystallography 2022
Materias:	Research Communications
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8819427/ https://www.ncbi.nlm.nih.gov/pubmed/35145744 http://dx.doi.org/10.1107/S2056989022000111

Ejemplares similares

N-N(+) Bond-Forming Intramolecular Cyclization of O-Tosyloxy β-Aminopropioamidoximes and Ion Exchange Reaction for the Synthesis of 2-Aminospiropyrazolilammonium Chlorides and Hexafluorophosphates
por: Kayukova, Lyudmila, et al.
Publicado: (2023)

2-Amino-5-ethoxycarbonyl-4-methylthiazol-3-ium chloride monohydrate
por: Lin, Jin Rui, et al.
Publicado: (2009)

2H-[1,3]Thiazolo[5,4,3-ij]quinolin-3-ium chloride monohydrate
por: Ehweiner, Madeleine A., et al.
Publicado: (2020)

Crystal structure of 2-amino-5-methylsulfanyl-1,3,4-thiadiazol-3-ium chloride monohydrate
por: Soudani, Sarra, et al.
Publicado: (2014)

6,7-Diphenyl-5-thia-7-azaspiro[2.6]nonan-8-one 5,5-dioxide
por: Yennawar, Hemant P., et al.
Publicado: (2023)

5-Fluoro-N-(2-methyl-3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-3-phenyl-1H-indole-2-carboxamide
por: Çelikesir, Sevim Türktekin, et al.
Publicado: (2013)

N-(3-Oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-6-phenylimidazo[2,1-b][1,3]thiazole-3-acetamide hemihydrate
por: Akkurt, Mehmet, et al.
Publicado: (2008)

6,7-Diphenyl-5-thia-7-azaspiro[2.6]nonan-8-one
por: Yennawar, Hemant P., et al.
Publicado: (2013)

N-[3-(4-Fluorobenzyl)-2,4-dioxo-1,3-diazaspiro[4.5]dec-8-yl]-2-methylbenzenesulfonamide
por: Jeyaseelan, S., et al.
Publicado: (2011)

4-Phenyl-1,2,4-triazaspiro[4.5]dec-1-ene-3-thione
por: Akkurt, Mehmet, et al.
Publicado: (2013)

N-(2,6-Dimethylanilino)-5,6-dihydro-4H-1,3-thiazin-3-ium chloride monohydrate
por: Veidis, Mikelis V., et al.
Publicado: (2008)

4-Benzyl-8-phenyl-1-thia-4-azaspiro[4.5]decan-3-one
por: Fun, Hoong-Kun, et al.
Publicado: (2012)

4-(Pyrimidin-2-yl)-1-thia-4-azaspiro[4.5]decan-3-one
por: Neuenfeldt, Patrícia D., et al.
Publicado: (2009)

8-Methyl-4-morpholinoethyl-1-thia-4-azaspiro[4.5]decan-3-one
por: Akkurt, Mehmet, et al.
Publicado: (2008)

Redetermination of dipotassium trichloridostannate(II) chloride monohydrate
por: Ye, Fei, et al.
Publicado: (2013)

N-(2,6-Dimethyl-3-oxo-1-thia-4-azaspiro[4.5]dec-4-yl)-2-hydroxy-2,2-diphenylacetamide
por: Yalçın, Şerife Pınar, et al.
Publicado: (2008)

Reaction Products of β-Aminopropioamidoximes Nitrobenzenesulfochlorination: Linear and Rearranged to Spiropyrazolinium Salts with Antidiabetic Activity
por: Kayukova, Lyudmila, et al.
Publicado: (2022)

N-(1-Acetyl-r-7,c-9-diphenyl-4,8-dithia-1,2-diazaspiro[5.4]dec-2-en-3-yl)acetamide
por: Gayathri, D., et al.
Publicado: (2008)

Phenazin-5-ium hydrogen sulfate monohydrate
por: deGeorge, Joseph, et al.
Publicado: (2013)

3-(4-Chlorophenyl)-7-methyl-4-(4-methylphenyl)-1-oxa-2,7-diazaspiro[4.5]dec-2-en-10-one
por: Gayathri, D., et al.
Publicado: (2008)

2-[2-(2,6-Dichloroanilino)phenyl]-N-[(2S)-2-methyl-3-oxo-8-phenyl-1-thia-4-azaspiro[4.5]dec-4-yl]acetamide
por: Akkurt, Mehmet, et al.
Publicado: (2010)

Redetermination of loperamide monohydrate
por: Jasinski, Jerry P., et al.
Publicado: (2012)

Boulton-Katritzky Rearrangement of 5-Substituted Phenyl-3-[2-(morpholin-1-yl)ethyl]-1,2,4-oxadiazoles as a Synthetic Path to Spiropyrazoline Benzoates and Chloride with Antitubercular Properties
por: Kayukova, Lyudmila, et al.
Publicado: (2021)

2-Amino-4-tert-butyl-5-(4-chlorobenzyl)thiazol-3-ium chloride
por: Peng, Jun-Mei, et al.
Publicado: (2010)

3-(4-Bromophenylsulfonyl)-8-methyl-1,3-diazaspiro[4.5]decane-2,4-dione
por: Kashif, M. Kalim, et al.
Publicado: (2009)

3-(4-Chlorophenylsulfonyl)-8-methyl-1,3-diazaspiro[4.5]decane-2,4-dione
por: Kashif, M. Kalim, et al.
Publicado: (2009)

7-Benzyl-2,7-diazaspiro[4.4]nonan-1-one
por: Guo, Huan-Mei
Publicado: (2011)

Redetermination of orotic acid monohydrate
por: Portalone, Gustavo
Publicado: (2008)

8-Ethyl-2-hydroxy-2-methyl-4-morpholinoethyl-1-thia-4-azaspiro[4.5]decan-3-one
por: Akkurt, Mehmet, et al.
Publicado: (2008)

rac-2-Hydroxy-2,8-dimethyl-4-morpholinoethyl-1-thia-4-azaspiro[4.5]decan-3-one
por: Akkurt, Mehmet, et al.
Publicado: (2008)

Privileged heterocycles: bioactivity and synthesis of 1,9-diazaspiro[5.5]undecane-containing compounds
por: Blanco-Ania, Daniel, et al.
Publicado: (2017)

Redetermination of the crystal structure of 2-oxo-1,3-thiazolidin-4-iminium chloride
por: Muthukkumar, Manickam, et al.
Publicado: (2019)

2,5-Dimethylanilinium chloride monohydrate
por: Smirani, Wajda, et al.
Publicado: (2008)

2,5-Dichloroanilinium chloride monohydrate
por: Gowda, B. Thimme, et al.
Publicado: (2009)

3,9-Diisopropyl-2,4,8,10-tetrathiaspiro[5.5]undecane
por: Gâz, Şerban Andrei, et al.
Publicado: (2010)

rac-Diethyl 9-hydroxy-9-methyl-7-phenyl-1,4-diazaspiro[4.5]decane-6,8-dicarboxylate
por: Maharramov, Abel M., et al.
Publicado: (2011)

Redetermination of 5-iodouracil
por: Portalone, Gustavo
Publicado: (2008)

3-(Piperidin-1-ium-1-yl)-6-azoniaspiro[5.5]undecane dibromide monohydrate
por: Gonzalez, Jorge, et al.
Publicado: (2011)

Anticonvulsant Profiles of Certain New 6-Aryl-9-substituted-6,9-diazaspiro-[4.5]decane-8,10-diones and 1-Aryl-4-substituted-1,4-diazaspiro[5.5]undecane-3,5-diones
por: Aboul-Enein, Mohamed N., et al.
Publicado: (2014)

Crystal structure and Hirshfeld surface analysis of 2-amino-5-{(1E)-1-[(carbamothioylamino)imino]ethyl}-4-methyl-1,3-thiazol-3-ium chloride monohydrate
por: Huseynov, Elnur Z., et al.
Publicado: (2023)

Cannot write session to /tmp/vufind_sessions/sess_oomqcqiprug36vedf7h4i2g0me