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Solid-state (17)O NMR study of α-d-glucose: exploring new frontiers in isotopic labeling, sensitivity enhancement, and NMR crystallography
We report synthesis and solid-state (17)O NMR characterization of α-d-glucose for which all six oxygen atoms are site-specifically (17)O-labeled. Solid-state (17)O NMR spectra were recorded for α-d-glucose/NaCl/H(2)O (2/1/1) cocrystals under static and magic-angle-spinning (MAS) conditions at five m...
| Autores principales: | , , , , , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
The Royal Society of Chemistry
2022
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8890099/ https://www.ncbi.nlm.nih.gov/pubmed/35340864 http://dx.doi.org/10.1039/d1sc06060k |