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Using diffraction losses of X-rays in a single crystal for determination of its lattice parameters as well as for monochromator calibration

A way has been developed to measure the unit-cell parameters of a single crystal just from an energy scan with X-rays, even when the exact energy of the X-rays is not well defined due to an error in the pitch angle of the monochromator. The precision of this measurement reaches da/a ∼ 1 × 10(−5). Th...

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Detalles Bibliográficos
Autores principales: Klimova, Nataliya, Snigireva, Irina, Snigirev, Anatoly, Yefanov, Oleksandr
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC8900831/
https://www.ncbi.nlm.nih.gov/pubmed/35254299
http://dx.doi.org/10.1107/S1600577521013667