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Single-Step Hydrolysis and Derivatization of Homocysteine Thiolactone Using Zone Fluidics: Simultaneous Analysis of Mixtures with Homocysteine Following Separation by Fluorosurfactant-Modified Gold Nanoparticles

Herein, we report a new automated flow method based on zone fluidics for the simultaneous determination of homocysteine and homocysteine thiolactone using fluorimetric detection (λ(ext) = 370 nm/λ(em) = 480 nm). Homocysteine thiolactone is hydrolyzed on-line in alkaline medium (1 mol L(−1) NaOH) to...

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Detalles Bibliográficos
Autores principales: Tsiasioti, Apostolia, Zacharis, Constantinos K., Tzanavaras, Paraskevas D.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9000217/
https://www.ncbi.nlm.nih.gov/pubmed/35408439
http://dx.doi.org/10.3390/molecules27072040