Cargando…

NMR Assignment of Methyl Groups in Immobilized Proteins Using Multiple-Bond (13)C Homonuclear Transfers, Proton Detection, and Very Fast MAS

In nuclear magnetic resonance spectroscopy of proteins, methyl protons play a particular role as extremely sensitive reporters on dynamics, allosteric effects, and protein–protein interactions, accessible even in high-molecular-weight systems approaching 1 MDa. The notorious issue of their chemical...

Descripción completa

Detalles Bibliográficos
Autores principales:	Paluch, Piotr, Augustyniak, Rafal, Org, Mai-Liis, Vanatalu, Kalju, Kaldma, Ats, Samoson, Ago, Stanek, Jan
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Frontiers Media S.A. 2022
Materias:	Molecular Biosciences
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9002630/ https://www.ncbi.nlm.nih.gov/pubmed/35425812 http://dx.doi.org/10.3389/fmolb.2022.828785

Ejemplares similares

Characterization of Protein–Protein Interfaces in Large Complexes by Solid-State NMR Solvent Paramagnetic Relaxation Enhancements
por: Öster, Carl, et al.
Publicado: (2017)

Spinning faster: protein NMR at MAS frequencies up to 126 kHz
por: Penzel, Susanne, et al.
Publicado: (2019)

T(2)* weighted Deconvolution of NMR Spectra: Application to 2D Homonuclear MAS Solid-State NMR of Membrane Proteins
por: V. S., Manu, et al.
Publicado: (2019)

Simplifying Proton NMR Spectra by Instant Homonuclear Broadband Decoupling(**)
por: Meyer, N Helge, et al.
Publicado: (2013)

Homonuclear Decoupling in (1)H NMR of Solids by Remote Correlation
por: Moutzouri, Pinelopi, et al.
Publicado: (2020)

High and fast: NMR protein–proton side-chain assignments at 160 kHz and 1.2 GHz
por: Callon, Morgane, et al.
Publicado: (2023)

Chemical shift transfer: an effective strategy for protein NMR assignment with ARTINA
por: Wetton, Henry, et al.
Publicado: (2023)

Simultaneous Assignment and Structure Determination of Proteins From Sparsely Labeled NMR Datasets
por: Mondal, Arup, et al.
Publicado: (2021)

Protein NMR Spectroscopy at 150 kHz Magic‐Angle Spinning Continues To Improve Resolution and Mass Sensitivity
por: Schledorn, Maarten, et al.
Publicado: (2020)

Simultaneous Broadband Suppression of Homonuclear and Heteronuclear Couplings in (1)H NMR Spectroscopy
por: Mycroft, Coral, et al.
Publicado: (2022)

100 kHz MAS Proton-Detected NMR Spectroscopy of Hepatitis B Virus Capsids
por: Lecoq, Lauriane, et al.
Publicado: (2019)

Homonuclear (1)H NMR and circular dichroism study of the HIV-1 Tat Eli variant
por: Watkins, Jennifer D, et al.
Publicado: (2008)

Optimal control theory enables homonuclear decoupling without Bloch–Siegert shifts in NMR spectroscopy
por: Coote, Paul W., et al.
Publicado: (2018)

Sensitivity enhancement of homonuclear multidimensional NMR correlations for labile sites in proteins, polysaccharides, and nucleic acids
por: Novakovic, Mihajlo, et al.
Publicado: (2020)

Strategies for RNA Resonance Assignment by (13)C/(15)N- and (1)H-Detected Solid-State NMR Spectroscopy
por: Aguion, Philipp Innig, et al.
Publicado: (2021)

Selective (1)H-(14)N Distance Measurements by (14)N Overtone Solid-State NMR Spectroscopy at Fast MAS
por: Duong, Nghia Tuan, et al.
Publicado: (2021)

Improved Detection and Quantification of Cyclopropane Fatty Acids via Homonuclear Decoupling Double Irradiation NMR Methods
por: Eltemur, Dilek, et al.
Publicado: (2023)

Assignment and secondary structure of the YadA membrane protein by solid-state MAS NMR
por: Shahid, Shakeel A., et al.
Publicado: (2012)

Optimisation of (1)H PMLG homonuclear decoupling at 60 kHz MAS to enable (15)N–(1)H through-bond heteronuclear correlation solid-state NMR spectroscopy
por: Tognetti, Jacqueline, et al.
Publicado: (2022)

Including Protons in Solid-State NMR Resonance Assignment and Secondary Structure Analysis: The Example of RNA Polymerase II Subunits Rpo4/7
por: Torosyan, Anahit, et al.
Publicado: (2019)

Heteronuclear and homonuclear radio-frequency-driven recoupling
por: Nimerovsky, Evgeny, et al.
Publicado: (2021)

A general method for diagonal peak suppression in homonuclear correlated NMR spectra by spatially and frequency selective pulses()
por: Glanzer, Simon, et al.
Publicado: (2013)

Correction: Optimisation of (1)H PMLG homonuclear decoupling at 60 kHz MAS to enable (15)N–(1)H through-bond heteronuclear correlation solid-state NMR spectroscopy
por: Tognetti, Jacqueline, et al.
Publicado: (2022)

Improved Magnetization Transfers among Quadrupolar Nuclei in Two-Dimensional Homonuclear Correlation NMR Experiments Applied to Inorganic Network Structures
por: Yu, Yang, et al.
Publicado: (2020)

Even harmonic generation in isotropic media of dissociating homonuclear molecules
por: Silva, R. E. F., et al.
Publicado: (2016)

PHRONESIS: A One‐Shot Approach for Sequential Assignment of Protein Resonances by Ultrafast MAS Solid‐State NMR Spectroscopy
por: Gopinath, Tata, et al.
Publicado: (2022)

Radiation damping strongly perturbs remote resonances in the presence of homonuclear mixing
por: Pelupessy, Philippe
Publicado: (2022)

Continuous in vivo Metabolism by NMR
por: Judge, Michael T., et al.
Publicado: (2019)

Determination of the primary structure and carboxyl pK(A)s of heparin-derived oligosaccharides by band-selective homonuclear-decoupled two-dimensional (1)H NMR
por: Nguyen, Khanh, et al.
Publicado: (2010)

NMR Studies of Tau Protein in Tauopathies
por: Kitoka, Kristine, et al.
Publicado: (2021)

Studying Metabolism by NMR-Based Metabolomics
por: Moco, Sofia
Publicado: (2022)

Contact replacement for NMR resonance assignment
por: Xiong, Fei, et al.
Publicado: (2008)

Retraction: Homonuclear bond activation using a stable N,N′-diamidocarbene
por: Wiggins, Kelly M., et al.
Publicado: (2015)

Algebraic Study of diatomic Molecules: homonuclear molecules H(2) and N(2)
por: Amiri, N., et al.
Publicado: (2020)

Modest Offset Difference Internuclear Selective Transfer via Homonuclear Dipolar Coupling
por: Nimerovsky, Evgeny, et al.
Publicado: (2022)

NMR Characterization of the Interactions Between Glycosaminoglycans and Proteins
por: Bu, Changkai, et al.
Publicado: (2021)

Medical Plants and Nutraceuticals for Amyloid-β Fibrillation Inhibition
por: Witter, Steffi, et al.
Publicado: (2018)

The Use of NMR to Study Transient Carbohydrate—Protein Interactions
por: Nieto, Pedro M.
Publicado: (2018)

NMR Methods for Structural Characterization of Protein-Protein Complexes
por: Purslow, Jeffrey A., et al.
Publicado: (2020)

Structural Biology in the Clouds: The WeNMR-EOSC Ecosystem
por: Honorato, Rodrigo V., et al.
Publicado: (2021)

Cannot write session to /tmp/vufind_sessions/sess_so99siluc3sd0vtvgp7bciu4dc