Proton-detected fast-magic-angle spinning NMR of paramagnetic inorganic solids

Fast (60 kHz) magic angle spinning solid-state NMR allows very sensitive proton detection in highly paramagnetic organometallic powders. We showcase this technique with the complete assignment of (1)H and (13)C resonances in a high-spin Fe(ii) polymerisation catalyst with less than 2 mg of sample at...

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Detalles Bibliográficos
Autores principales: Blahut, Jan, Benda, Ladislav, Lejeune, Arthur L., Sanders, Kevin J., Burcher, Benjamin, Jeanneau, Erwann, Proriol, David, Catita, Leonor, Breuil, Pierre-Alain R., Quoineaud, Anne-Agathe, Pell, Andrew J., Pintacuda, Guido
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2021
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9040908/
https://www.ncbi.nlm.nih.gov/pubmed/35479571
http://dx.doi.org/10.1039/d1ra04110j

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9040908/
https://www.ncbi.nlm.nih.gov/pubmed/35479571
http://dx.doi.org/10.1039/d1ra04110j

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