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Efficient syntheses of macrocycles ranging from 22–28 atoms through spontaneous dimerization to yield bis-hydrazones

Acid treatment of a triazine displaying both a tethered acetal and BOC-protected hydrazine group leads to spontaneous condensation to yield macrocyclic dimers in excellent yields and purity. The bis-triazinyl hydrazones that form are characterized by (1)H-NMR, (13)C-NMR, (1)H-COSY spectroscopy, X-ra...

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Detalles Bibliográficos
Autores principales: Sharma, Vishal R., Mehmood, Arshad, Janesko, Benjamin G., Simanek, Eric E.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9048830/
https://www.ncbi.nlm.nih.gov/pubmed/35497724
http://dx.doi.org/10.1039/c9ra08056b