A structure determination protocol based on combined analysis of 3D-ED data, powder XRD data, solid-state NMR data and DFT-D calculations reveals the structure of a new polymorph of l-tyrosine

We report the crystal structure of a new polymorph of l-tyrosine (denoted the β polymorph), prepared by crystallization from the gas phase following vacuum sublimation. Structure determination was carried out by combined analysis of three-dimensional electron diffraction (3D-ED) data and powder X-ra...

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Detalles Bibliográficos
Autores principales: Smalley, Christopher J. H., Hoskyns, Harriet E., Hughes, Colan E., Johnstone, Duncan N., Willhammar, Tom, Young, Mark T., Pickard, Christopher J., Logsdail, Andrew J., Midgley, Paul A., Harris, Kenneth D. M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2022
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9093151/
https://www.ncbi.nlm.nih.gov/pubmed/35655549
http://dx.doi.org/10.1039/d1sc06467c

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9093151/
https://www.ncbi.nlm.nih.gov/pubmed/35655549
http://dx.doi.org/10.1039/d1sc06467c

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