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Synthesis, crystal structure, and properties of methyl-substituted coronene amide analogue

A coronene amide analogue was synthesized in six steps using an improved method at the final biarylation step. The key to the progress of palladium-mediated biarylation involved the introduction of three methyl groups to suppress the undesired reaction and the use of tri-tert-butylphosphine as the l...

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Detalles Bibliográficos
Autores principales: Rakumitsu, Kenta, Fujii, Miho, Kusumoto, Sotaro, Kikkawa, Shoko, Azumaya, Isao, Yokoyama, Akihiro
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9479769/
https://www.ncbi.nlm.nih.gov/pubmed/36275098
http://dx.doi.org/10.1039/d2ra04035b