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Synthesis, crystal structure and Hirshfeld surface analysis of tert-butyl N-acetylcarbamate
This article reports a practical synthesis of tert-butyl acetylcarbamate, C(7)H(13)NO(3), from N-Boc-thioacetamide and the study of its crystal structure. The reaction proceeds in the presence of natural phosphate as a catalyst, with excellent yield, simple workup and benign environment. The cryst...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9535831/ https://www.ncbi.nlm.nih.gov/pubmed/36250123 http://dx.doi.org/10.1107/S2056989022009483 |