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Determination of Total Sennosides and Sennosides A, B, and A(1) in Senna Leaflets, Pods, and Tablets by Two-Dimensional qNMR

In the present work, a two-dimensional qNMR method for the determination of sennosides was established. Using band-selective HSQC and the cross correlations of the characteristic 10–10’ bonds, we quantified the total amount of the value-determining dianthranoids in five minutes, thus, rendering the...

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Detalles Bibliográficos
Autores principales: Çiçek, Serhat Sezai, Moreno Cardenas, Calisto, Girreser, Ulrich
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9656819/
https://www.ncbi.nlm.nih.gov/pubmed/36364175
http://dx.doi.org/10.3390/molecules27217349