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Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching

In this paper, we reported on wafer-scale nanoporous (NP) AlGaN-based deep ultraviolet (DUV) distributed Bragg reflectors (DBRs) with 95% reflectivity at 280 nm, using epitaxial periodically stacked n-Al(0.62)Ga(0.38)N/u-Al(0.62)Ga(0.38)N structures grown on AlN/sapphire templates via metal–organic...

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Autores principales: Zhao, Yongming, Shan, Maocheng, Zheng, Zhihua, Jian, Pengcheng, Liu, WeiJie, Tan, Shizhou, Chen, Changqing, Wu, Feng, Dai, Jiangnan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9794686/
https://www.ncbi.nlm.nih.gov/pubmed/36575216
http://dx.doi.org/10.1038/s41598-022-25712-2
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author Zhao, Yongming
Shan, Maocheng
Zheng, Zhihua
Jian, Pengcheng
Liu, WeiJie
Tan, Shizhou
Chen, Changqing
Wu, Feng
Dai, Jiangnan
author_facet Zhao, Yongming
Shan, Maocheng
Zheng, Zhihua
Jian, Pengcheng
Liu, WeiJie
Tan, Shizhou
Chen, Changqing
Wu, Feng
Dai, Jiangnan
author_sort Zhao, Yongming
collection PubMed
description In this paper, we reported on wafer-scale nanoporous (NP) AlGaN-based deep ultraviolet (DUV) distributed Bragg reflectors (DBRs) with 95% reflectivity at 280 nm, using epitaxial periodically stacked n-Al(0.62)Ga(0.38)N/u-Al(0.62)Ga(0.38)N structures grown on AlN/sapphire templates via metal–organic chemical vapor deposition (MOCVD). The DBRs were fabricated by a simple one-step selective wet etching in heated KOH aqueous solution. To study the influence of the temperature of KOH electrolyte on the nanopores formation, the amount of charge consumed during etching process was counted, and the surface and cross-sectional morphology of DBRs were characterized by Scanning electron microscopy (SEM) and atomic force microscopy (AFM). As the electrolyte temperature increased, the nanopores became larger while the amount of charge reduced, which revealed that the etching process was a combination of electrochemical and chemical etching. The triangular nanopores and hexagonal pits further confirmed the chemical etching processes. Our work demonstrated a simple wet etching to fabricate high reflective DBRs, which would be useful for AlGaN based DUV devices with microcavity structures.
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spelling pubmed-97946862022-12-29 Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching Zhao, Yongming Shan, Maocheng Zheng, Zhihua Jian, Pengcheng Liu, WeiJie Tan, Shizhou Chen, Changqing Wu, Feng Dai, Jiangnan Sci Rep Article In this paper, we reported on wafer-scale nanoporous (NP) AlGaN-based deep ultraviolet (DUV) distributed Bragg reflectors (DBRs) with 95% reflectivity at 280 nm, using epitaxial periodically stacked n-Al(0.62)Ga(0.38)N/u-Al(0.62)Ga(0.38)N structures grown on AlN/sapphire templates via metal–organic chemical vapor deposition (MOCVD). The DBRs were fabricated by a simple one-step selective wet etching in heated KOH aqueous solution. To study the influence of the temperature of KOH electrolyte on the nanopores formation, the amount of charge consumed during etching process was counted, and the surface and cross-sectional morphology of DBRs were characterized by Scanning electron microscopy (SEM) and atomic force microscopy (AFM). As the electrolyte temperature increased, the nanopores became larger while the amount of charge reduced, which revealed that the etching process was a combination of electrochemical and chemical etching. The triangular nanopores and hexagonal pits further confirmed the chemical etching processes. Our work demonstrated a simple wet etching to fabricate high reflective DBRs, which would be useful for AlGaN based DUV devices with microcavity structures. Nature Publishing Group UK 2022-12-27 /pmc/articles/PMC9794686/ /pubmed/36575216 http://dx.doi.org/10.1038/s41598-022-25712-2 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Zhao, Yongming
Shan, Maocheng
Zheng, Zhihua
Jian, Pengcheng
Liu, WeiJie
Tan, Shizhou
Chen, Changqing
Wu, Feng
Dai, Jiangnan
Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title_full Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title_fullStr Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title_full_unstemmed Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title_short Fabrication of wafer-scale nanoporous AlGaN-based deep ultraviolet distributed Bragg reflectors via one-step selective wet etching
title_sort fabrication of wafer-scale nanoporous algan-based deep ultraviolet distributed bragg reflectors via one-step selective wet etching
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9794686/
https://www.ncbi.nlm.nih.gov/pubmed/36575216
http://dx.doi.org/10.1038/s41598-022-25712-2
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