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Specimen-displacement correction for powder X-ray diffraction in Debye–Scherrer geometry with a flat area detector

The effect of small changes in the speci­men-to-detector distance on the unit-cell parameters is examined for synchrotron powder diffraction in Debye–Scherrer (transmission) geometry with a flat area detector. An analytical correction equation is proposed to fix the shift in 2θ values due to speci­m...

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Detalles Bibliográficos
Autores principales: Hulbert, Benjamin S., Kriven, Waltraud M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9901925/
https://www.ncbi.nlm.nih.gov/pubmed/36777137
http://dx.doi.org/10.1107/S1600576722011360