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Specimen-displacement correction for powder X-ray diffraction in Debye–Scherrer geometry with a flat area detector
The effect of small changes in the specimen-to-detector distance on the unit-cell parameters is examined for synchrotron powder diffraction in Debye–Scherrer (transmission) geometry with a flat area detector. An analytical correction equation is proposed to fix the shift in 2θ values due to specim...
Autores principales: | Hulbert, Benjamin S., Kriven, Waltraud M. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9901925/ https://www.ncbi.nlm.nih.gov/pubmed/36777137 http://dx.doi.org/10.1107/S1600576722011360 |
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