Pentafluoropropionic Anhydride Derivatization and GC-MS Analysis of Histamine, Agmatine, Putrescine, and Spermidine: Effects of Solvents and Starting Column Temperature

Gas chromatography–mass spectrometry (GC-MS) is useful for the quantitative determination of the polyamines spermidine (SPD) and putrescine (PUT) and of the biogenic amine agmatine (AGM) in biological samples after derivatization. This GC-MS method involves a two-step extraction with n-butanol and h...

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Detalles Bibliográficos
Autores principales: Tsikas, Dimitrios, Beckmann, Bibiana, Baskal, Svetlana, Brunner, Gorig
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9920471/
https://www.ncbi.nlm.nih.gov/pubmed/36770607
http://dx.doi.org/10.3390/molecules28030939

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9920471/
https://www.ncbi.nlm.nih.gov/pubmed/36770607
http://dx.doi.org/10.3390/molecules28030939

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